A rotary evaporator is able to distill solvents more quickly at lower temperatures through the use of a vacuum. Distillation using semi-microscale apparatus. The jointless design eliminates the need to fit pieces together. The pear-shaped flask allows the last drop of residue to be removed, compared with a similarly-sized round-bottom flask ...
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Get DetailsApr 01, 2015 Article Deviations from Beer's law on the microscale ... The construction of an inexpensive rotary evaporator. ... R. V. Hoffman. Rotary evaporators are needed in a number of pedagogically ...
Get DetailsAug 11, 2021 Then the mixture was dried by a rotary evaporator. The dried mixture was subjected to pyrolysis treatment at 800 C under N 2 atmosphere for 2 …
Get DetailsCobb's Red Cabbage Indicator.. ERIC Educational Resources Information Center. Cobb, Vicki. 1998-01-01. Describes the use of an indicator made from the pigment in red cabbage. Cabbage is grated then soaked in water. When the water is a strong red, the cabbage is strained out. The cabbage-juice indicator is then used to test for acids and bases. Includes a list of good foods …
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Get DetailsJan 08, 2019 The solvent was removed by rotary evaporation. Device fabrication A dextran (09184, Sigma-Aldrich) aqueous solution (5 wt%) was spin coated on a …
Get DetailsMar 05, 2021 5.2D: Microscale Distillation; ... A rotary evaporator is essentially a reduced pressure distillation: a solution in a round bottomed flask is placed in the water bath of the apparatus, and rotated while the system is partially evacuated (by a water aspirator or vacuum pump). The reduced pressure in the apparatus causes the solvent to boil at a ...
Get DetailsMar 06, 2022 Separating proteins from their mixtures is an important process in a great variety of applications, but it faces difficult challenges as soon as the proteins are simultaneously of similar sizes and carry comparable net charges. To develop both efficient and sustainable strategies for the selective separation of similar proteins and to understand the underlying molecular …
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Get DetailsSep 27, 2021 Undesired layers can be properly disposed of when the desired compound is in your hands (e.g. after the rotary evaporator has removed the solvent). ... Microscale Extractions. Microscale work involves the manipulation of less than \(300 \: \text{mg}\) of compound, and usually involves solvent volumes of \(5 \: \text{mL}\) or less. A separatory ...
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