A cooling bath or ice bath, in laboratory chemistry practice, is a liquid mixture which is used to maintain low temperatures, typically between 13 C and −196 C.These low temperatures are used to collect liquids after distillation, to remove solvents using a rotary evaporator, or to perform a chemical reaction below room temperature (see Kinetic control).
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Get DetailsOct 17, 2012 Cooling was carried out at room temperature for 30 min. Solvent was removed by rotary evaporator and further by heating at 50 C under vacuum overnight. The resulting uncured powder sample was ...
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Get DetailsSep 21, 2020 After removing the solvent on a rotary evaporator, the mixture was purified by column chromatography using DCM:hexane (1:3, v/v) as the eluent to …
Get DetailsThe liquid fraction was evaporated at atmospheric pressure by a rotary evaporator with a water bath at 85 C to recover the oil. The total yields of gas product as well as loss during collection, separation, and extraction grouped together as “gas + loss” and calculated by …
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